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Title: | Iodine-Mediated, Microwave-Assisted Synthesis of 1-Arylnaphthofurans via Cyclization of 1-(1′-Arylvinyl)-2-naphthols |
Authors: | Kumar, Anil |
Keywords: | Chemistry Iodine-mediated Microwave-assisted Hydroarylation 1-arylnaphthofurans one-pot reaction |
Issue Date: | 2015 |
Publisher: | Thieme |
Abstract: | A metal-free, one-pot, iodine-mediated, microwave-assisted cyclization of 1-(1′-arylvinyl)-2-naphthols (ortho-vinylnaphthols) into 1-arylnaphthofurans is developed. The 1-arylnaphthofurans are isolated in good to excellent yields (65–90%) using two equivalents of iodine in acetonitrile. The reactions proceed via the formation of 1-(2-iodo-1-phenylvinyl)naphthalen-2-ols as intermediates. Overall, the protocol is convenient as the reactions occur smoothly without the requirement of a transition-metal catalyst. |
URI: | https://www.thieme-connect.com/products/ejournals/abstract/10.1055/s-0035-1560268 http://dspace.bits-pilani.ac.in:8080/xmlui/handle/123456789/2856 |
Appears in Collections: | Department of Chemistry |
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