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Title: | Synthesis of Ionic Liquid-Supported Sulfonyl Azide and Its Application in Diazotransfer Reaction |
Authors: | Kumar, Anil |
Keywords: | Chemistry Salts Azides Reagents Chemical reactions Solvents |
Issue Date: | 2012 |
Publisher: | ACS |
Abstract: | The paper describes synthesis of a novel ionic liquid-supported sulfonyl azide and its applications as diazotransfer reagent of active methylene compounds as well as deformylative diazo transfer reagent. The diazo compounds were isolated in excellent yields (82–94%) and high purity. The method offers better separation of product and reagent. This method is experimentally simple and mild, and requires very short reaction time. |
URI: | https://pubs.acs.org/doi/10.1021/jo301529b http://dspace.bits-pilani.ac.in:8080/xmlui/handle/123456789/2917 |
Appears in Collections: | Department of Chemistry |
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