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http://dspace.bits-pilani.ac.in:8080/jspui/xmlui/handle/123456789/3080| Title: | Facile One‐Step Conversion of Ketones into α‐Azidoketones using [Hydroxy(tosyloxy)iodo]benzene and Sodium Azide in the Presence of a Phase‐Transfer Catalyst under Solvent‐Free Conditions |
| Authors: | Kumar, Dalip |
| Keywords: | Chemistry α‐Azidoketone Phase‐transfer catalyst Solvent‐free synthesis |
| Issue Date: | Dec-2005 |
| Publisher: | Taylor & Francis |
| Abstract: | We have described a one‐step, solvent‐free synthesis of α‐azidoketones from the corresponding ketones that requires relatively benign [hydroxy(tosyloxy) iodo]‐benzene reagent, sodium azide, and phase‐transfer catalyst at room temperature. Generality of the protocol has been demonstrated by synthesizing various α‐azidoketones high in yield and purity within a short time. |
| URI: | https://www.tandfonline.com/doi/full/10.1080/00397910600602644 http://dspace.bits-pilani.ac.in:8080/xmlui/handle/123456789/3080 |
| Appears in Collections: | Department of Chemistry |
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