Browsing by Author "Robertson, Andrew J. B"
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Item Detection and Identification of Organic Radicals Produced in the Low Pressure Silent Electric Discharge by an Electron Spin Resonance Spin Trapping Technique(Journal of the Chemical Society : Faraday Transaction - I. The Chemical Society, London. 1977, 73 (10), 1977) Hibbert, D. Brynn; Robertson, Andrew J. B; Perkins, M. JohnA method is described whereby free radicals are produced in a low pressure silent electric discharge between glass surfaces and are simultaneously deposited with 2-methyl-2-nitrosopropane as a spin trap on a cold surface. The resulting deposit is warmed to room temperature and subjected to electron spin resonance examination. A variety of alkyl and other radicals were trapped with different reactants in the discharge tube.