An efficient PTT-mediated synthesis of a-azidoketones in ionic liquids

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Date

2011-08

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NISCAIR

Abstract

A simple and efficient one-pot method has been described for the direct synthesis of ⍺-azidoketones from various ketones possess­ing ⍺-hydrogen by reaction with phenyltrimethyl­ammo­nium tribromide (PTT) and subsequent treatment with NaN3 in ionic liquid. The procedure gives high yield and the ionic liquid can be reused.

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Chemistry, Phenyltrimethylammonium tribromide (PTT), TMSN, Bromoazidation

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https://www.google.com/url?sa=t&rct=j&q=&esrc=s&source=web&cd=&ved=2ahUKEwiozZeNrNbzAhVaWH0KHTknDPAQFnoECAQQAQ&url=http%3A%2F%2Fnopr.niscair.res.in%2Fbitstream%2F123456789%2F12517%2F1%2FIJCB%252050B%25288%2529%25201123-1127.pdf&usg=AOvVaw3Ez0-x6TYWTlK8EB8IyPz4
 http://dspace.bits-pilani.ac.in:8080/xmlui/handle/123456789/2946

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Department of Chemistry

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